Synthesis, X-ray Characterisation and St
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Constantinos D. Antoniadis; Sotiris K. Hadjikakou; Nick Hadjiliadis; Maciej Kubi
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Article
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2004
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John Wiley and Sons
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English
⚖ 144 KB
## Abstract The reaction of 2‐mercaptopyridine (C~5~H~5~NS or PYSH) with diiodine in a molar ratio of 1:2 in dichloromethane led to the oxidation and dimerization of the ligand and formation of [(PYS−PYSH)^+^·I~3~^−^]. The compound was characterised by elemental analysis, DTA‐TG, FT‐Raman, FT‐IR, U