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Synthesis and Characterization of Organolanthanide Complexes with a Calix[4]-pyrrolyl Ligand and Their Catalytic Activities toward Hydrophosphonylation of Aldehydes and Unactivated Ketones

✍ Scribed by Zhou, Shuangliu; Wang, Hengyu; Ping, Jian; Wang, Shaowu; Zhang, Lijun; Zhu, Xiancui; Wei, Yun; Wang, Fenhua; Feng, Zhijun; Gu, Xiaoxia

Book ID: 111957937
Publisher: American Chemical Society
Year: 2012
Tongue: English
Weight: 690 KB
Volume: 31
Category: Article
ISSN: 0276-7333
DOI: 10.1021/om2008925

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## Abstract New mononuclear titanium complexes [TiCl(Rcalix)] [R = Me (1), Bz (2), SiMe~3~ (3)] supported by __p__‐__tert__‐butylcalix[4]arene mono(organyl)ethers (Rcalix) were prepared in good yield from H~2~R~2~calix and [TiCl~4~(THF)~2~]. The crystallographically characterized complex [TiCl(Meca