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SYNTHESIS AND CHARACTERIZATION OF NEW OXODIPEROXOVANADATE COMPLEXES CONTAINING COORDINATED AMINOACIDS

✍ Scribed by Gerbase, A. E.; Martinelli, M.; Fagundes, L. G.; Stefani, V.; Da Silva, S. J.

Book ID
127003423
Publisher
Taylor and Francis Group
Year
1999
Tongue
English
Weight
453 KB
Volume
47
Category
Article
ISSN
0095-8972

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The reaction of the lithium Ξ²-diketoiminate complex (dipp with ZnCl 2 yielded the corresponding (dipp)NacNacZnCl ( 1) and (dipp)NacNacZn(Β΅-Cl) 2 Li(OEt 2 ) 2 (1a). Treatment of 1 with LiCΟ΅CPh and NaBH 4 in diethyl ether gave (dipp)Nac-NacZnCΟ΅CPh ( 2) and (dipp)NacNacZn(Β΅-H) 2 BH 2 (3). The core ele