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Synthesis and characterization of molybdenum and tungsten nitrite complexes of the type [M(NO2)2(CO)2(PPh3)2]

✍ Scribed by Robert D. Feltham; Edward Rajaseelan

Publisher
Elsevier Science
Year
1994
Tongue
English
Weight
258 KB
Volume
218
Category
Article
ISSN
0020-1693

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## Abstract Treatment of [OsCl~2~(PPh~3~)~3~] with HC≡CR (R = Ph, __p__‐tolyl, CMe~3~) in the presence of HCl gives the corresponding trichloro(carbyne) complexes [OsCl~3~(≡CCH~2~R)(PPh~3~)~2~] in good yields. The vinylidene complexes [OsCl~2~(=C=CHR)(PPh~3~)~2~] (R = Ph, __p__‐tolyl, CMe~3~) are,