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Synthesis and characterization of magnesium doped lead titanate

✍ Scribed by F. Z. Fadil; T. Lamcharfi; F. Abdi; M. Aillerie

Publisher
John Wiley and Sons
Year
2011
Tongue
English
Weight
284 KB
Volume
46
Category
Article
ISSN
0232-1300

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✦ Synopsis

Abstract

Magnesium (Mg) doped lead titanate powders (PT: Mg) ceramics, with various Mg contents (0, 2.5, 5, 7.5, 10, 12.5, 15, 17.5, 20, and 30 mole %), are prepared by the sol‐gel method and characterized by X‐Ray diffraction (XRD), scanning electron microscopy (SEM) and Raman spectroscopy. XRD results show that the magnesium diminishes the lattice tetragonality of PT:Mg. The average particle size and morphology were studied by SEM. The investigations done by Raman spectroscopy allow the analyzis of the substitution mechanism behavior related to the Mg incorporation into PT structure. A concentration threshold appears around 10% of Mg corresponding in a change of the compensation process with Mg^2+^ ions replacing Pb^2+^ ions below and both Pb^2+^ and Ti^4+^ above. (Β© 2011 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)

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