Synthesis and characterization of diphenylmethyltin(IV) mono-, di-, and trichloroacetate
✍ Scribed by Mostafa Mohammadpour Amini; Mohammad Yousefi
- Publisher
- John Wiley and Sons
- Year
- 2003
- Tongue
- English
- Weight
- 74 KB
- Volume
- 14
- Category
- Article
- ISSN
- 1042-7163
- DOI
- 10.1002/hc.10059
No coin nor oath required. For personal study only.
✦ Synopsis
Abstract
Diphenylmethyltin(IV) mono‐, di‐, and trichloroacetate have been synthesized and characterized by infrared, ^1^H, ^13^C, ^119^Sn NMR, and mass spectroscopy. Infrared spectroscopy indicates that the prepared organotin carboxylates possess chain polymer structures. NMR data show that the mono‐ and dichloro derivatives do not retain the solid state structure in solution. © 2003 Wiley Periodicals, Inc. Heteroatom Chem 14:18–22, 2003; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.10059
📜 SIMILAR VOLUMES
## Abstract β‐Cryptoxanthin (1) was acetylated and then epoxidized with monoperoxyphthalic acid. After hydrolysis, repeated chromatography, and crystallization, (3__S__,5__R__,6__S__)‐5,6‐epoxy‐β‐cryptoxanthin (3), (3__S__,5__S__,6__R__)‐5,6‐epoxy‐β‐cryptoxanthin (4), (3__R__,5′__R__,6′__R__)‐5′,6′