✦ LIBER ✦

Synthesis and characterization of conducting copolymer of (N1,N3-bis(thiophene-3-ylmethylene)benzene-1,3-diamine-co-3,4-ethylenedioxythiophene)

✍ Scribed by Altuğ Kümbül; Ersen Turaç; Tuğba Dursun; Ertuğrul Şahmetlioğlu

Book ID: 111491302
Publisher: Versita
Year: 2010
Tongue: English
Weight: 374 KB
Volume: 64
Category: Article
ISSN: 0366-6352
DOI: 10.2478/s11696-009-0087-6

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✦ Synopsis

Abstract

Electrochemical copolymerization of N 1,N 3-bis(thiophene-3-ylmethylene)benzene-1,3-diamine (TMBA) with 3,4-ethylenedioxythiophene (EDOT) was carried out in a CH3CN/LiClO4 (0.1 M) solvent-electrolyte via potentiodynamic electrolysis. Chemical structure of the monomer was determined by nuclear magnetic resonance (1H NMR) and Fourier transform infrared (FTIR) spectroscopy. The resulting copolymer was characterized by cyclic voltammetry (CV), FTIR, scanning electron microscopy (SEM), and thermogravimetry analyses (TGA). Conductivity measurements of the copolymer and PEDOT (poly(3,4-ethylenedioxythiophene)) were carried out by the four-probe technique.

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