✦ LIBER ✦

Synthesis and Characterization of an Organically Templated Lamellar Vanadium–Gallium Phosphate, [NH3(CH2)2NH3]4[Ga4–xVx(HPO4)5(PO4)3H(OH)2](x=1.65)

✍ Scribed by Ann M. Chippindale; Andrew R. Cowley

Publisher: Elsevier Science
Year: 2001
Tongue: English
Weight: 576 KB
Volume: 159
Category: Article
ISSN: 0022-4596
DOI: 10.1006/jssc.2001.9130

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✦ Synopsis

A new two-dimensional vanadium+gallium phosphate (VGaPO), [NH 3 (CH 2 ) 2 NH 3 ] 4 [Ga 4؊x V x (HPO 4 ) 5 (PO 4 ) 3 H(OH) 2 ] (x ‫؍‬ 1.65), has been synthesized under solvothermal conditions at 433 K in the presence of ethylenediamine and the structure determined using room-temperature single-crystal X-ray di4raction data (M r ‫؍‬ 1296.22, triclinic, space group P؊1; a ‫؍‬ 9.991(1),

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