Synthesis and characterization of aluminophosphate molecular sieve AlPO4-41 from alcohol systems
β Scribed by Qiuming Gao; Jiesheng Chen; Shougui Li; Ruren Xu
- Publisher
- Elsevier Science
- Year
- 1996
- Tongue
- English
- Weight
- 286 KB
- Volume
- 7
- Category
- Article
- ISSN
- 0927-6513
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β¦ Synopsis
The full crystallization of the aluminophosphate form of the AFO (A1PO4-41) structure was realized, for the first time, from non-aqueous systems involving an alcohol as the solvent. Several secondary amines including diethylamine, dipropylamine, diisopropylamine, dibutylamine and dipentylamine were used as the templates to direct the formation of this molecular sieve. The products were characterized by X-ray powder diffraction, scanning electron microscopy, differential thermal analysis, and thermogravimetric analysis.
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## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a βFull Textβ option. The original article is trackable v
AlPO,-H2 is a microporous hydrated aluminophosphate, structurally related to VPIS, whose framework has highly elliptical lo-ring channels (2.9 x 7.6 A) parallel to the c crystallographic axis. To resolve a previously reported discrepancy between nuclear magnetic resonance (NMR) and X-ray diffraction