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Synthesis and Characterization of a New Chromanoisoxazole (II).

✍ Scribed by Y. L. N. Murthy; Rani Nanda; K. Ravi Kumar; G. Y. S. K. Swamy


Publisher
John Wiley and Sons
Year
2006
Weight
12 KB
Volume
37
Category
Article
ISSN
0931-7597

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The reaction of [NBu(4)](2)[Ni(C(6)F(5))(4)] (1) with solutions of dry HCl(g) in Et(2)O results in the protonolysis of two Nibond;C(6)F(5) bonds giving [NBu(4)](2)[[Ni(C(6)F(5))(2)](2)(mu-Cl)(2)] (2 a) together with the stoichiometrically required amount of C(6)F(5)H. Compound 2 a reacts with AgClO(