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Synthesis and Characterization of a Mercury-Intercalated Molybdenum Disulfide

✍ Scribed by S. Lemaux; A.S. Golub; P. Gressier; G. Ouvrard

Publisher
Elsevier Science
Year
1999
Tongue
English
Weight
123 KB
Volume
147
Category
Article
ISSN
0022-4596

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✦ Synopsis

Elemental mercury cannot be intercalated into crystalline molybdenum disul5de as such, probably for structural reasons, the a parameter of the host being too small. On the contrary, we show that a reaction between restacked MoS 2 and liquid mercury allows the synthesis of such an intercalate. X-ray absorption spectroscopy experiments show that such di4erent behavior is due to the appropriate structural con5guration of the restacked phase. Intercalated mercury stabilizes the structural and d 3 electronic con5guration of molybdenum.

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