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Synthesis and Characterization of a Boron-Aluminum Oxochloride

✍ Scribed by Jihong Yu; Ruren Xu; Yihua Xu; Yong Yue

Book ID: 102605456
Publisher: Elsevier Science
Year: 1996
Tongue: English
Weight: 255 KB
Volume: 122
Category: Article
ISSN: 0022-4596
DOI: 10.1006/jssc.1996.0102

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The diborane(4) derivatives Mes,BB(Mes)Ph and Me,N(Ph)BB(Ph)NMe, readily react with lithium powder in ether to give the doubly reduced salts [{(Et,O)Li},Mes,,BB(Mes)Ph] and [{(EtzO)Li}~Me,N(Ph)BB(Ph)NMe~]. Both species, which were isolated as red crystals, have been characterized by X-ray crystallog