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Synthesis and characterization of 1,9-difluoro-5-methyl-5-phenyl-10,11-dihydro-5H-dibenzo[b,f]silepin

✍ Scribed by Joyce Y. Corey; Alexander J. Pitts; Rudolph E.K. Winter; Nigam P. Rath

Publisher: Elsevier Science
Year: 1995
Tongue: English
Weight: 772 KB
Volume: 499
Category: Article
ISSN: 0022-328X
DOI: 10.1016/0022-328x(95)00326-l

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## Abstract magnified image Reactions of 3‐chlorobenzo[__b__]thiophene‐2‐carbonyl chloride with 2‐alkyl‐2‐aminopropanamides have been used to prepare a series of carboxamides **1a‐d** (yields 61‐85%). The products were submitted to base‐catalysed ring closure reactions to give the corresponding 4,