Synthesis and characterization of 1,4-dichlorospiropentadiene

✍ Scribed by Rajesh K. Saini; Vladislav A. Litosh; Andrew D. Daniels; W.E. Billups

• Book ID: 104262076
• Publisher: Elsevier Science
• Year: 1999
• Tongue: French
• Weight: 85 KB
• Volume: 40
• Category: Article
• ISSN: 0040-4039
• DOI: 10.1016/s0040-4039(99)01293-9

✦ Synopsis

1,4-Dichlorospiropentadiene was prepared by vacuum gas-sofid elimination of compound 3 over solid (n-Bu)4N + F" and characterized by IH and 13C NMR spectroscopy at -103 °C.