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Synthesis and Biological Evaluation of Tetrahydroisoquinolin-4-ol Derivatives

✍ Scribed by Williams, LR; Quessy, SN


Book ID
111975628
Publisher
Commonwealth Scientific and Industrial Research Organisation Publishing
Year
1979
Tongue
English
Weight
562 KB
Volume
32
Category
Article
ISSN
0004-9425

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mixture was poured into ice-water(l00 ml) and extracted with CHC13(100 ml x 3). The extract was washed with H20, dried over MgS04 and evaporated to give Z-methylpropyl phenyl ketone(5d) as an oil(l6.20 g, 94%). 'H-NMR: 8.00(2H,dd,J=8.5 and 1.5Hz1, 7.60-7.23 (3H,m), 2.84(2H,d, J=6.8Hz), 2.40-2.08(lH,