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Synthesis and biological activity of the dihydrotachysterol2 metabolite 25-hydroxydihydrotachysterol2

✍ Scribed by Maestro, Miguel A.; Castedo, L.; Mouriño, A.; Rookhuizen, Rob B.; Bosch, R.; Norman, A.W.

Book ID
122632327
Publisher
Elsevier Science
Year
1992
Tongue
English
Weight
179 KB
Volume
43
Category
Article
ISSN
0960-0760

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25-hydroxydihydrotachysterol2 an innovat
25-hydroxydihydrotachysterol2 an innovative synthesis of a key metabolite of dihydrotachysterol2
✍ Jaap C. Hanekamp; Rob Boer Rookhuizen; Hendrik J.T. Bos; Lambert Brandsma 📂 Article 📅 1992 🏛 Elsevier Science 🌐 French ⚖ 898 KB

A new synthesis of 25-hydroxydihydrotachysterol2 is described. The hydroxylated side-chain is constructed stereoselectively using a chiral Wittig reagent. The A-ring synthon is introduced utilising the Wittig-Homer method as developed by Lythgoe et al. The preparation of the metabolite is carried ou