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Synthesis and biological activity of some thioglycidyl and thietanyl esters of pentavalent phosphorus acids

✍ Scribed by B. A. Arbuzov; O. N. Nuretdinova; I. D. Neklesova; I. S. Iraidova; M. A. Kudrina; N. V. Egorova

Book ID: 112421720
Publisher: Springer
Year: 1971
Tongue: English
Weight: 275 KB
Volume: 20
Category: Article
ISSN: 1573-9171
DOI: 10.1007/bf00851256

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A mixture of 12.5 g of 2,2-dimethyl-l,3-dioxolan and 25 ml of glacial acetic acid is added to 10 grams of addition product (3). The mixture is then stirred and heated to 60°C. The diazonium salt dissolves, and after 10 minutes, the reaction is completed. After working up as described above, 89.3 % o