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Synthesis and biological activity of 10-thia-10-deaza analogs of folic acid, pteroic acid, and related compounds

✍ Scribed by Kim, Y. H.; Gaumont, Y.; Kisliuk, R. L.; Mautner, H. G.

Book ID: 126105911
Publisher: American Chemical Society
Year: 1975
Tongue: English
Weight: 612 KB
Volume: 18
Category: Article
ISSN: 0022-2623
DOI: 10.1021/jm00242a002

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## Abstract The folate analogue, 9‐thia‐5,10‐dideazafolic acid (**3b**), was obtained in an efficient two‐step procedure in an overall yield of 60%. The previously unknown intermediate dimethyl‐thiocarbamic acid S‐(2‐amino‐3,4‐dihydo‐4‐oxo‐pyrido[2,3‐__d__]pyrimidin‐6‐yl) ester (**5**) was prepared