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Synthesis and application of cationic 2,6-bis(2-oxazolinyl)phenylpalladium(II) complexes

✍ Scribed by Mark A Stark; Christopher J Richards

Publisher: Elsevier Science
Year: 1997
Tongue: French
Weight: 212 KB
Volume: 38
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(97)01309-9

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✦ Synopsis

Treatment of 1,3-bis(2-oxatzolinyl)benzenes with LDA/TMEDA followed by the addition of PdBr2(1,5-COD) gave 2,6-bis(2-oxazolinyl)phenylbromopalladium(II) complexes. Subsequent bromide abstraction with silver salts provided a series cationic 2,6-bis(2-oxazolinyl)phenylpalladium(II) complexes that effectively catalyse the addition of ct-cyano carboxylates to methyl vinyl ketone.

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