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Synthesis and analysis of the C1C18 alkyl oleates

✍ Scribed by Corinne Vieville; Zéphirin Mouloungui; Antoine Gaset

Book ID
103037062
Publisher
Elsevier Science
Year
1995
Tongue
English
Weight
423 KB
Volume
75
Category
Article
ISSN
0009-3084

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✦ Synopsis

The C~-CI8 alkyl oleates were prepared in n-hexane by esterification of oleic acid with either the primary and secondary Ct-C 6 alcohols or the primary fatty C8-C~8 alcohols. The esterification was acid-catalyzed in the presence of p-toluene sulfonic acid (p-TSA) in a pseudo-homogeneous phase, or in the presence of the sulfonic macroporous resin (K2411) in the heterogeneous phase. The purified alkyl oleates were characterized by 13C-NMR. The oleic acid/alkyl oleate mixtures were analyzed by high-performance liquid chromatography (HPLC).

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