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Synthesis, AM1calculation, and biological studies of thiopyran-4-one and their azine derivatives

✍ Scribed by J. Jayabharathi; V. Thanikachalam; A. Thangamani; M. Padmavathy

Book ID
105770800
Publisher
Springer-Verlag
Year
2007
Tongue
English
Weight
324 KB
Volume
16
Category
Article
ISSN
1054-2523

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Starting from tetrahydrothiopyran-4-one (4d) a rational NMR spectra, redox behavior, and crystal structure (H 4 -3a and 3a). The very low solubility of 3a and 3b prevented eight-step synthesis of 3a has been developed with 25 % overall yield. This route passes H 4 -3a and H 2 -3a which are further r