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Synthesis, 13C NMR spectrum and crystal structure of 10-Phenylpyrido[3,2-b][1,4]benzothiazine 5-Oxide

✍ Scribed by Misa V. Jovanovic; Edward R. Biehl; Patrice De Meester; Shirley S. C. Chu


Book ID
112128234
Publisher
Journal of Heterocyclic Chemistry
Year
1986
Tongue
English
Weight
305 KB
Volume
23
Category
Article
ISSN
0022-152X

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From the crude product of the synthesis of the dithiadiphosphetane [RP(S)S], (with R = 2,4,6-iPr3C,H,), the trans-oxathiadiphosphetane RIS)P P(S)R has been isolated, C.,,,H,,OP,S,. X-ray structure analysis and mass spectroscopic investigations give unequivocal evidence for this structure: monoclinic