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Syntheses, structure and rare earth metal photoluminescence of new and known isostructural A2Mo4Sb2O18 (A=Ce, Pr, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu) compounds

✍ Scribed by Shrikant A. Mohitkar; G. Kalpana; K. Vidyasagar

Publisher: Elsevier Science
Year: 2011
Tongue: English
Weight: 848 KB
Volume: 184
Category: Article
ISSN: 0022-4596
DOI: 10.1016/j.jssc.2011.01.008

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✦ Synopsis

Nine new A 2 Mo 4 Sb 2 O 18 (A¼ Ce, Pr, Eu, Tb, Ho, Er, Tm, Yb, Lu) compounds have been synthesized by solid-state reactions. They are isostructural with six reported analogues of yttrium and other lanthanides and the monoclinic unit cell parameters of all fifteen of them vary linearly with the size of A 3 + ion. Single crystal X-ray structures of eight A 2 Mo 4 Sb 2 O 18 (A ¼Ce, Pr, Eu, Gd, Tb, Ho, Er, Tm) compounds have been determined. Neat A 2 Mo 4 Sb 2 O 18 (A ¼Pr, Sm, Eu, Tb, Dy, Ho, Er, Tm) compounds exhibit characteristic rare earth metal photoluminescence.

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