𝔖 Bobbio Scriptorium
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Syntheses of large-ring bis-indolic dilactams

✍ Scribed by Catherine Charlet-Fagnère; Wei-Qun Jiang; Jean-Yves Laronze

Book ID
104260863
Publisher
Elsevier Science
Year
1999
Tongue
French
Weight
270 KB
Volume
40
Category
Article
ISSN
0040-4039

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✦ Synopsis

~fteen maetocycles ranging from 11 to 26 atoms, containing two tryptamine units connected by an aeyl chain between the N(b) and N(b') atoms and a (poly)methylene linker (or a bond) between C(2) or C(6'), were prepared by two different procedures.

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Two robust, efficient syntheses of [phenyl ring-U-14 C]indole are presented. In the first synthesis, we developed optimum reaction conditions for the Houben-Hoesch alkylation of chloro acetonitrile with aniline. This was found through the screening of several Lewis acids coupled with the use of Suga