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Syntheses of l-rubranitrose (2,3,6-trideoxy-3-C-methyl-4-O-methyl-3-nitro-l-xylo-hexopyranose) and the naturally occurring d enantiomer

โœ Scribed by John S. Brimacombe; Khandker M.M. Rahman

Publisher
Elsevier Science
Year
1983
Tongue
English
Weight
132 KB
Volume
114
Category
Article
ISSN
0008-6215

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ChemInform Abstract: Studies of the Synt
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โœ H. YE; L. NOECKER; W. J. BOYKO; R. M. GIULIANO; G. P. A. YAP; A. L. RHEINGOLD ๐Ÿ“‚ Article ๐Ÿ“… 2010 ๐Ÿ› John Wiley and Sons โš– 31 KB ๐Ÿ‘ 2 views

Studies of the Synthesis of Rubranitrose and Crystal Structure of Methyl 2,3,6-Trideoxy-3-C-methyl-3-nitro-ฮฑ-D-ribo-hexopyranoside. -The title hexopyranoside (II) is investigated as a precursor to D-rubranitrose, a nitro sugar found in the antibiotic rubradirin. -(YE, H.; NOECKER,

Conformational difference in the solid s
Conformational difference in the solid state and in solution of methyl 2,3,4-trideoxy-2,4-di-C-methyl-6-O-trityl-ฮฑ-d-lyxo-hexopyranoside
โœ Masataka Mori; Tatsuji Chuman; Takane Fujimori; Kunio Kato; Akira Ohkubo; Shozo ๐Ÿ“‚ Article ๐Ÿ“… 1984 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 479 KB

The conformational difference of the title compound (1) in the solid state and in solution has been investigated by X-ray crystallography and high-field proton n.m.r. spectrometry. In the solid state, compound 1 adopts the "c,(D) conformation (la), whereas 1 exists preferentially in the 'C4(D) confo