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Syntheses of isotopically labelled L-α-amino acids with an asymmetric centre at C-3

✍ Scribed by Harding, John R.; Hughes, Rachael A.; Kelly, Nicholas M.; Sutherland, Andrew; Wilis, Christine L.

Book ID
121228423
Publisher
Royal Society of Chemistry
Year
2000
Weight
194 KB
Volume
20
Category
Article
ISSN
1472-7781

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Stereoselective Synthesis of Stable Isotope Labeled L-α-Amino Acids: Synthesis of L−[4−13C] and L−[3,4−13C2]Aspartic Acid
✍ Siegfried N. Lodwig; Clifford J. Unkefer 📂 Article 📅 1992 🏛 John Wiley and Sons 🌐 French ⚖ 542 KB

## Abstract We have developed a stereoselective route to isotopically labeled L‐aspartic acid using L‐serine as a chiral precursor. Labeled serine, prepared biosynthetically was N‐protected by conversion to the N‐__t__‐Boc derivative. (N‐__t__‐Boc)‐[3−^13^C]Serine is cyclized to its β‐lactone which