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Syntheses of (C8H8)Ln(C9H7) · (THF)2(Ln = Pr,Nd) and crystal structure of (C8H8)Pr(C9H7) · (THF)2

✍ Scribed by Ke Wen; Zhong-Sheng Jin; Ge-Cheng Wei; Wen-Qi Chen

Book ID: 112060083
Publisher: John Wiley and Sons
Year: 2010
Tongue: English
Weight: 318 KB
Volume: 10
Category: Article
ISSN: 0256-7660
DOI: 10.1002/cjoc.19920100407

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LiNPPh 3 reacts with the cyclooctatetraenide complexes [Ln(C 8 H 8 )Cl(THF) 2 ] 2 of cerium and samarium in tetrahydrofuran solution forming the phosphorane iminato complexes [Ln(C 8 H 8 )Li 3 Cl 2 (NPPh 3 ) 2 (THF) 3 ]. According to crystal structure analyses these complexes show heterocubane struc