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Syntheses of 24R,25-dihydroxy-[6,19,19-3H]vitamin D3 and 24R,25-dihydroxy-[6,19,19-2H]vitamin D3

โœ Scribed by Sachiko Yamada; Masato Shimizu; Kenji Fukushima; Koichi Niimura; Yuji Maeda


Book ID
116065420
Publisher
Elsevier Science
Year
1989
Tongue
English
Weight
595 KB
Volume
54
Category
Article
ISSN
0039-128X

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Synthesis of a C-24-epimeric mixture of 25-hydroxy-[26,27-3H]vitamin D2 and a C-24-epimeric mixture of 1,25-dihydroxy-[26,27-'HIvitamin D2 by the Grignard reaction of the corresponding 25-keto-27-nor-vitamin D2 and lo-acetoxy-25keto-27-nor-vitamin D3 with tritiated methyl magnesium bromide is descri