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Syntheses of 2,4-diaryl-2,3-dihydro-1,5-benzothiazepines

✍ Scribed by Alan R. Katritzky; Boris V. Rogovoy; Christophe Chassaing; Vladimir Vvedensky; Behrouz Forood; Brenton Flatt; Hisao Nakai

Publisher: Journal of Heterocyclic Chemistry
Year: 2000
Tongue: English
Weight: 290 KB
Volume: 37
Category: Article
ISSN: 0022-152X
DOI: 10.1002/jhet.5570370642

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✦ Synopsis

Abstract

The condensation of α,β‐unsaturated ketones with substituted o‐aminothiophenols, obtained by reductive cleavage of the corresponding disulfides in the presence of triphenylphosphine, is an effective method for the synthesis of 2,4‐diaryl‐2,3‐dihydro‐1,5‐benzothiazepines under neutral conditions.

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