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Syntheses in the benzo[2,1,3]thiadiazole series

โœ Scribed by F. S. Mikhailitsyn


Book ID
112441479
Publisher
Springer US
Year
1973
Tongue
English
Weight
310 KB
Volume
9
Category
Article
ISSN
0009-3122

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Disulfides of the benzo-2,1,3-thiadiazol
โœ I. A. Belen'kaya; T. A. Shulla ๐Ÿ“‚ Article ๐Ÿ“… 1989 ๐Ÿ› Springer US ๐ŸŒ English โš– 457 KB

A solution of 1 g (0.012 mole) of sodium nitrite in i0 ml of water was added to a hot solution of 2.7 g (0.01 mole) of 3-phenyl-4,5-dichloro-l,2,3-thiadiazolium chloride in 20 ml of 50% ethanol. The darkyellow precipitate was filtered, and recrystallized from a benzene-heptane (I:I) mixture. Yield,