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Syntheses, crystal structures, and optical properties of K3V0.32Ta0.68S4, K6Nb1.07Ta2.93S22, K6Nb2.97Ta1.03S25, K3Cu3Nb0.98Ta1.02S8, and KCu2Nb0.53Ta0.47S4

✍ Scribed by Yuandong Wu; Wolfgang Bensch

Publisher
Elsevier Science
Year
2007
Tongue
English
Weight
915 KB
Volume
180
Category
Article
ISSN
0022-4596

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The title compounds were prepared from the elements by reactions in sealed tantalum tubes in a high-frequency furnace. Their structures were re5ned from single crystal X-ray di4ractometer data: Pnma, a ‫؍‬ 744.4(1) pm, b ‫؍‬ 434.15(9) pm, c ‫؍‬ 845.5(1) pm, wR2 ‫؍‬ 0.0433, 658 F 2 values, 20 variabl