Syntheses and structures of silver(I) complexes of 4-amino-3,5-dimethyl-4H-1,2,4-triazole and 4-amino-3,5-diethyl-4H-1,2,4-triazole: role of the substituents
β Scribed by Guang Yang; Ying-Li Wang; Li-Li Liu; Seik Weng Ng
- Publisher
- Springer
- Year
- 2009
- Tongue
- English
- Weight
- 457 KB
- Volume
- 34
- Category
- Article
- ISSN
- 0340-4285
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π SIMILAR VOLUMES
The Schiff bases 3a-h obtained from 4-amino-1,2,4-triazol-3-ones 1a-h when subjected to Japp-Klingemann reaction yielded the corresponding 3-{2-[(2-aryl-5-methyl-3H-[1,2,4]-triazol-3-one-4-yl)]-iminophenyl}-pentane-2,4-diones 4 a-h. These diones on cyclisation with N 2 H 4 yielded the title compound
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## Abstract A simple and efficient method for the preparation of triazolesulfonic acids (II) is presented.