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Syntheses and Spectroscopic and Structural Characterization of Molybdenum(VI) Citrato Monomeric Raceme and Dimer, K 4 [MoO 3 (cit)]·2H 2 O and K 4 [(MoO 2 ) 2 O(Hcit) 2 ]·4H 2 O

✍ Scribed by Zhou, Zhao-Hui; Wan, Hui-Lin; Tsai, Khi-Rui

Book ID
120446223
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
99 KB
Volume
39
Category
Article
ISSN
0020-1669

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Synthesis, characterization and crystal
Synthesis, characterization and crystal structures of three dinuclear diperoxo complexes of Mo(VI): K2{O[MoO(O2)2H2O]2}·2H2O, (C6H8N,NH4){O[MoO(O2)2H2O]2} and (C6H8N,Na){O[MoO(O2)2H2O]2}
✍ M. Grzywa; W. Nitek; W. Łasocha 📂 Article 📅 2008 🏛 Elsevier Science 🌐 English ⚖ 526 KB

The crystal structures of three dinuclear diperoxo compounds have been determined from single-crystal X-ray diffraction data. All title compounds crystallize as yellow needle-shaped crystals in the triclinic space group P 1(2). ( 1 where 2-MepyH denotes 2-methylopyridine, crystallize with a = 6.733