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Syntheses and Properties of Graphyne Fragments: Trigonally Expanded Dehydrobenzo[12]annulenes

✍ Scribed by Tahara, Kazukuni; Yamamoto, Yuki; Gross, Dustin E.; Kozuma, Hiroyoshi; Arikuma, Yoko; Ohta, Koji; Koizumi, Yoshiko; Gao, Yuan; Shimizu, Yo; Seki, Shu; Kamada, Kenji; Moore, Jeffrey S.; Tobe, Yoshito

Book ID: 120533739
Publisher: John Wiley and Sons
Year: 2013
Tongue: English
Weight: 820 KB
Volume: 19
Category: Article
ISSN: 0947-6539
DOI: 10.1002/chem.201300838

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## Abstract To develop a novel π‐conjugated molecule‐based supramolecular assembly, we designed and synthesized trisdehydrotribenzo[12]annulene ([12]DBA) derivative **2** with three carboxyl groups at the periphery. Recrystallization of **2** from DMSO gave a crystal of the solvate **2⋅**3 DMSO. Cr