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Syntheses and characterizations of iridium complexes containing bidentate phosphine ligands and their catalytic hydrogenation reactions to α,β-unsaturated aldehydes

✍ Scribed by Rui-Xiang Li; Xian-Jun Li; Ning-Bew Wong; Kam-Chung Tin; Zhong-Yuan Zhou; Thomas C.W Mak

Publisher: Elsevier Science
Year: 2002
Tongue: English
Weight: 150 KB
Volume: 178
Category: Article
ISSN: 1381-1169
DOI: 10.1016/s1381-1169(01)00294-1

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## Abstract The enantiopure complexes **3a** and **3b** [Rh(NBD)(P,S)]^+^BF~4~^−^ [P,S = (__S__)‐2‐(diphenylphosphanyl)‐2′‐(methylthio)‐1,1′‐binaphthalene (**a**); (__S__)‐2‐(diphenylphosphanyl)‐2′‐(isopropylthio)‐1,1′‐binaphthalene (**b**)] have been prepared from [Rh(NBD)(THF)~2~]^+^BF~4~^−^ by r