Synthesis of trans/syn- and trans/anti-D
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Dipl.-Chem. P. Richter; Prof. Dr. E. Fahr
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Article
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1969
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John Wiley and Sons
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English
⚖ 197 KB
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The reaction products were fractionated in a 2-mpackedcolumn. (2a) + (2b) (z 1 :l), b.p. 74-74.5 'C,%O torr, n: = 1.4898. (2a) + (26) stillcontained 4 % of cis,cis-l,3-cyclooctadiene. This additional compound can be detected gas chromatographically only after hydrogenation. (3), b.p. 67 "CjlOO torr,