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Synthese d'Acide Benzisoxazole-1, 2 Acetique-3 (14C-α) et (14c-β)

✍ Scribed by P. Thourel; J. P. Noel; J. P. Beaucourt

Publisher
John Wiley and Sons
Year
1988
Tongue
French
Weight
355 KB
Volume
25
Category
Article
ISSN
0022-2135

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✦ Synopsis

Service der Ilol&culer )I.rqu&er CXN-SACLAY 91191 GIF-SUR-WETTE CEDKX M I SIII+UBY I The preparations of 1.~-bcnsiroxaso~e-3-.c.tic acid labelled with 14C in porition a o r B of the ride chain are dercribed. a-14C acid war obtained from 4-hydroxy cormrarin [3-14C] via Prier rearrangewnt of phenyl acetate [methyl-B -l4C acid war ryntherized from 4-hydroxy comarin [Z-14C] obtained from "C-diethy1 carbonate. Labelled poritionr were determined by purr spectrometry and were in agreem8nt with the propored reaction rchew . 14 C].

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