Synthesis of trans/syn- and trans/anti-D
โ
Dipl.-Chem. P. Richter; Prof. Dr. E. Fahr
๐
Article
๐
1969
๐
John Wiley and Sons
๐
English
โ 197 KB
๐ 1 views
The reaction products were fractionated in a 2-mpackedcolumn. (2a) + (2b) (z 1 :l), b.p. 74-74.5 'C,%O torr, n: = 1.4898. (2a) + (26) stillcontained 4 % of cis,cis-l,3-cyclooctadiene. This additional compound can be detected gas chromatographically only after hydrogenation. (3), b.p. 67 "CjlOO torr,