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syn- and anti-forms of Benzil Monodimethylhydrazone

โœ Scribed by William L. Collibee; James P. Springer; Byron H. Arison; J.-P. Anselme


Publisher
Wiley (John Wiley & Sons)
Year
2010
Weight
122 KB
Volume
100
Category
Article
ISSN
0037-9646

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Synthesis of trans/syn- and trans/anti-D
โœ Dipl.-Chem. P. Richter; Prof. Dr. E. Fahr ๐Ÿ“‚ Article ๐Ÿ“… 1969 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 197 KB ๐Ÿ‘ 1 views

The reaction products were fractionated in a 2-mpackedcolumn. (2a) + (2b) (z 1 :l), b.p. 74-74.5 'C,%O torr, n: = 1.4898. (2a) + (26) stillcontained 4 % of cis,cis-l,3-cyclooctadiene. This additional compound can be detected gas chromatographically only after hydrogenation. (3), b.p. 67 "CjlOO torr,