Symmetry principles for the design of radiofrequency pulse sequences in the nuclear magnetic resonance of rotating solids
✍ Scribed by Marina Carravetta; Mattias Edén; Xin Zhao; Andreas Brinkmann; Malcolm H Levitt
- Book ID
- 108311871
- Publisher
- Elsevier Science
- Year
- 2000
- Tongue
- English
- Weight
- 226 KB
- Volume
- 321
- Category
- Article
- ISSN
- 0009-2614
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A new radiofrequency pulse sequence is introduced for the efficient reintroduction of magnetic dipolar couplings in the magic-angle-spinning NMR of solids. The sequence involves seven phase-shifted radiofrequency pulse cycles, timed to span two rotational periods of the sample. Double-quantum cohere
## Abstract Until quite recently dilatation measurements were frequently used to provide information related to the solid phase content of commercial shortenings and margarine fats. With the appearance of reliable and relatively inexpensive pulsed magnetic resonance spectrometers it has become poss