Symmetry and magnetic structure determination: developments in refinement techniques and examples
β Scribed by A.S. Wills
- Book ID
- 106024328
- Publisher
- Springer
- Year
- 2002
- Tongue
- English
- Weight
- 63 KB
- Volume
- 74
- Category
- Article
- ISSN
- 1432-0630
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π SIMILAR VOLUMES
Fe4(P2O7)3 was prepared from Fe(PO3)3 and FePO4 at 9403C under oxygen. The unit cell is monoclinic, space group P21"n, with a β«Ψβ¬ 7.389(2) A > , b β«Ψβ¬ 21.337(1) A > , c β«Ψβ¬ 9.517(2) A > , β«Ψβ¬ 90(1)3, and Z β«Ψβ¬ 4. The crystallographic structure has been determined from a single crystal through direct
C+Fe(PO 3 ) 3 has been synthesized using H 3 PO 4 and Fe(NO 3 ) 3 ' 9H 2 O as starting compounds. Single crystals were grown under vacuum with a trace of FeCl 2 . Fe(PO 3 ) 3 crystallizes in the monoclinic space group Cc, with a β«Ψβ¬ 13.148(4) A s , b β«Ψβ¬ 19.076(2) A s , c β«Ψβ¬ 9.410(3) A s , β«Ψβ¬ 127.