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Suzuki–Miyaura Cross-Coupling and Ring-Closing Metathesis: A Strategic Combination for the Synthesis of Cyclophane Derivatives

✍ Scribed by Sambasivarao Kotha; Kalyaneswar Mandal

Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
152 KB
Volume
2006
Category
Article
ISSN
1434-193X

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✦ Synopsis

Abstract

The synthesis of cyclophane derivatives through a sequence involving Suzuki–Miyaura cross‐coupling between α,α′‐dibromo‐m‐xylene and arylboronic acid derivatives, alkenylation and ring‐closing metathesis has been achieved. One of the cyclophanes was obtained by tandem isomerization and metathesis. Significant magnetic anisotropic effects on the intra‐annular hydrogen atoms were observed. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2006)

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