Surface reactions and the effects of oxygen on Pb atomization in graphite furnace atomic absorption spectrometry
β Scribed by James A. Holcombe; Maureen S. Droessler
- Book ID
- 112321672
- Publisher
- Springer
- Year
- 1986
- Tongue
- English
- Weight
- 822 KB
- Volume
- 323
- Category
- Article
- ISSN
- 1618-2650
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Palladium was determined in pharmaceuticals by direct graphite furnace atomic absorption spectrometry (GFAAS) method. The detection limit was 0.1 mg/g in 5% solution; the recovery of 0.5-2.0 mg/g Pd spike was close to 100%. The flow injection GFAAS method was worked out using oxime and iminodiacetic
A procedure was developed for the quanhficatlon of thalbum at the ultratrace level (ng g-l) m geoloacal matenals The sample 1s dissolved m 3 M H2S04 to which IS added KI and K,HP04 The thalhum IS then extracted as its mdo complex mto methyhsobutyl ketone (MIBK), leavmg behind most of the n-on The re