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Supramolecular Polymers Generated from Heterocomplementary Monomers Linked through Multiple Hydrogen-Bonding Arrays—Formation, Characterization, and Properties

✍ Scribed by Volker Berl; Marc Schmutz; Michael J. Krische; Richard G. Khoury; Jean-Marie Lehn


Publisher
John Wiley and Sons
Year
2002
Tongue
English
Weight
581 KB
Volume
8
Category
Article
ISSN
0947-6539

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✦ Synopsis


Supramolecular polymers are described that are derived from the association of two homoditopic heterocomplementary monomers through sextuple hydrogen-bonding arrays. They form fibers and a variety of different materials depending on the conditions. The strong affinity of the DAD ± DAD (D donor, A acceptor) hydrogenbonding sites for double-faced cyanuric acid type wedges drives the supramolec-ular polymeric assembly in apolar and chlorinated organic solvents. The marked influence of stoichiometry, as well as end-capping and cross-linking agents upon fiber formation is revealed in solution and by electron microscopy (EM). The results further contribute to the development of a supramolecular polymer chemistry that comprizes reversible polymers formed through recognition-controlled noncovalent connections between the molecular components. Such materials are, by nature, dynamic and present adaptive character in view of their ability to respond to external stimuli.