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Supramolecular Assemblies of Mononuclear and Polymeric Nickel(II) Glutarato Complexes via π-π Stacking Interactions and Hydrogen Bonds: [Ni(H2O)3(phen)(C5H6O4)] · H2O and [Ni(H2O)2(phen)(C5H6O4)]

✍ Scribed by Jian-Li Lin; Yue-Qing Zheng; Zu-Ping Kon; Hong-Liang Zhang

Publisher
John Wiley and Sons
Year
2001
Tongue
German
Weight
192 KB
Volume
627
Category
Article
ISSN
0372-7874

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Cu(C 12 H 8 N 2 )(C 4 H 4 O 4 )(H 2 O)] 2 ´C4 H 6 O 4 was prepared by the reaction of succinic acid, CuCl 2 ´2 H 2 O, 1,10-phenanthroline (phen = C 12 H 8 N 2 ), and Na 2 CO 3 in a CH 3 OH±H 2 O solution. The crystal structure (triclinic, P 1 (no. 2), a = 7.493(1), b = 9.758(1), c = 13.517(1) A Ê ;

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Blue crystals of Cu 2 (phen) 2 (H 2 O) 2 (C 5 H 6 O 4 ) 2 were obtained from a CH 3 OH±H 2 O solution containing CuCl 2 , 1,10-phenanthroline (phen), glutaric acid and Na 2 CO 3 . The crystal structure (monoclinic, P2 1 /c (no. 14), a = 10.271(1), b = 10.595(1), c = 15.585(1) A Ê , b = 107.105(3)°,