The magnitudes and relative signs of 13C-'% and 'H-'% coupling constants in 6-F-indole, 5-and 6-F-tryptamine, 5-F-indole-3-carboxaldehyde, 2and 4-F-biphenyl, droperidol, flusperilene, l-F-naphthalene and 3-F-fluroanthene (F = fluoro) have been determined using two-dimensional % -' H chemical shift c
β¦ LIBER β¦
Suppression of homonuclear J couplings in 1H-13C chemical-shift correlation maps
β Scribed by V Rutar
- Publisher
- Elsevier Science
- Year
- 1984
- Weight
- 259 KB
- Volume
- 58
- Category
- Article
- ISSN
- 0022-2364
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## Three different two-dimensional "C-'H shift-correlation sequences which detect 'H chemical shifts and one bond '3C-'H[J(CH)I couplings in f, with full 'H-'H decoupling are described and evaluated. They are particularly useful for detecting small differences in 'J(CH) for nonquivalent methylene