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Suppression of Crazing in Polystyrene Crosslinked with a Multifunctional Zirconium Oxo Cluster Observed In Situ during Tensile Tests

✍ Scribed by Stephan Puchegger; Harald Rennhofer; Franz Rene Kogler; Dieter Loidl; Sigrid Bernstorff; Ulrich Schubert; Herwig Peterlik


Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
246 KB
Volume
28
Category
Article
ISSN
1022-1336

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✦ Synopsis


Abstract

The structural development of polystyrene, which was crosslinked with varying amounts of the multifunctional cluster Zr~6~O~4~(OH)~4~(methacrylate)~12~, was followed in situ by small‐angle X‐ray scattering at a synchrotron radiation source. It was observed that crazing strongly diminishes with increasing cluster proportion and disappears nearly completely for the material with the highest cluster proportion of 0.87 mol‐%. Accordingly, the maximum stress before failure is strongly enhanced, whereas the maximum strain decreases.

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