A pilot plant was designed and used to extract cumin seeds (Cuminum cyminum L.) using supercritical carbon dioxide at 408C and 100 bar. The extracts obtained were compared with cumin essential oil obtained by conventional steam distillation, using GC±MS. The analyses show that valuable components ar
Supercritical carbon dioxide extraction of okra (Hibiscus esculentus L) seeds
✍ Scribed by Csaba D András; Béla Simándi; Ferenc Örsi; Charalambos Lambrou; Doukeni Missopolinou-Tatala; Costas Panayiotou; János Domokos; Fruzsina Doleschall
- Publisher
- John Wiley and Sons
- Year
- 2005
- Tongue
- English
- Weight
- 177 KB
- Volume
- 85
- Category
- Article
- ISSN
- 0022-5142
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✦ Synopsis
Abstract
Pilot‐scale supercritical fluid extraction of okra seeds was carried out, using carbon dioxide as solvent, at temperatures of 40, 50 and 60 °C and pressures of 150, 300 and 450 bar. Laboratory‐scale Soxhlet extraction of the ground seeds was carried out with ethanol and n‐hexane. The yields of supercritical fluid extraction and n‐hexane Soxhlet extractions were similar. The ethanol Soxhlet extraction gave the highest yield, but the concentrations of β‐sitosterol and tocopherols in this extract were lower than in the supercritical fluid extraction product. The fatty acid profiles of the extracts were determined, and a high unsaturated/saturated ratio was observed. The fatty acid compositions were only slightly different for oils obtained by the different extraction methods. Copyright © 2005 Society of Chemical Industry
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