Highly precise and accurate sulphur analyses are required to establish material balance for sulphur in utility boilers where sulphur is present at low levels in the fly ashes. Sulphur determinations using the established methods depend on quantitative extraction of sulphur from some form of sample d
Sulphur in coal
โ Scribed by Armstrong, V. ;Himus, G. W.
- Publisher
- Wiley (John Wiley & Sons)
- Year
- 1939
- Weight
- 682 KB
- Volume
- 58
- Category
- Article
- ISSN
- 0368-4075
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A controlled-atmosphere, programmed-temperature, oxidation apparatus has been constructed and used to characterize organic-sulphur distribution in coals, partially desulphurized coals, and model systems. Samples were diluted with WO, and heated, in a stream of Ar containing 10% 02, at a programmed-t
The ASTM method for the analysis of sulphur forms in coal is applied to a hydrodesutphurized coal. Precautions necessary to prevent the calculation of erroneous high values of organic sulphur are illustrated. The reduction of sulphate ion to sulphite ion by the hydrogen is reported. A complete sulph