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Sulfur-Nitrogen Compounds. III. The Acid Hydrolysis of Hydroxylamine N,N-Disulfonate and Hydroxylamine N- and O-Monosulfonates 1

✍ Scribed by Candlin, J. P.; Wilkins, R. G.

Book ID
126437421
Publisher
American Chemical Society
Year
1965
Tongue
English
Weight
537 KB
Volume
87
Category
Article
ISSN
0002-7863

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## Abstract C^14^‐labelled O,N‐dimethylhydroxyurethane is synthesized from C^14^‐labelled dimethylsulfate and N‐hydroxy‐urethane. It is further converted without purification into O,N‐^14^‐C‐dimethyl‐hydroxylammoniumchloride, which was then nitrosated with sodiumnitrite in acidic medium to give N‐N