Assignment of the 1H and 13C signals arising from the carbohydrate portion of sucrose octabenzoate has been achieved using homonuclear shift correlation experiments (COSY) and one-bond 1H-13C heteronuclear shift correlation measurements, respectively. The 13C resonances of the carbonyl carbon atoms
Sucrose: An Assignment of the 13 C N.M.R. Parameters by Selective Decoupling
β Scribed by Jones, AJ; Hanisch, P; McPhail, AK
- Book ID
- 121696935
- Publisher
- Commonwealth Scientific and Industrial Research Organisation Publishing
- Year
- 1979
- Tongue
- English
- Weight
- 144 KB
- Volume
- 32
- Category
- Article
- ISSN
- 0004-9425
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π SIMILAR VOLUMES
## Abstract Characteristic differences in multiplet hyperfine structure observed in coupled ^13^C n.m.r. spectra of symmetrical __o__βdisubstituted benzene rings are explained on general grounds. Contrary to earlier proposals, the observation of this effect in unsymmetrical systems is not a suitabl
## Abstract The ^13^C n.m.r. spectrum of mutarotated Dβribose is completely assigned by using 2β and 3βdeuterioβDβribose as reference compounds. The signal intensities of the largely relaxed ^13^C n.m.r. spectrum are evaluated, and the equilibrium mixture of mutarotated Dβribose is found to consist